Commission Regulation (EC) No 152/2009 of 27 January 2009 laying down the methods... (32009R0152)
Commission Regulation (EC) No 152/2009 of 27 January 2009 laying down the methods of sampling and analysis for the official control of feed (Text with EEA relevance)
- COMMISSION REGULATION (EC)
- No 152/2009
- of 27 January 2009
- laying down the methods of sampling and analysis for the official control of feed
- (Text with EEA relevance)
- Article 1
- Article 2
- Article 3
- Article 4
- Article 5
- Article 6
- Article 7
- ANNEX I
- METHODS OF SAMPLING
- 1. PURPOSE AND SCOPE
- 2. SAMPLING PERSONNEL
- 3. DEFINITIONS
- 4. APPARATUS
- 4.2. Apparatus recommended for the sampling of solid feed.
- 4.2.1. Manual sampling
- 4.2.2. Mechanical sampling
- 4.2.3. Divider
- 5. QUANTITATIVE REQUIREMENTS
- 6. INSTRUCTIONS FOR TAKING, PREPARING AND PACKAGING THE SAMPLES
- 6.1. General
- 6.2. Incremental samples
- 6.2.A. In relation to the control of substances or products uniformly distributed throughout the feed
- 6.2.A.1.
- Loose feed
- 6.2.A.2.
- Packaged feed
- 6.2.A.3.
- Homogeneous or homogenisable liquid or semi-liquid feed
- 6.2.A.4.
- Non-homogenisable, liquid or semi-liquid feed
- 6.2.A.5.
- Feed blocks and mineral licks
- 6.2.B. In relation to the control of undesirable substances or products likely to be distributed non-uniformly throughout the feed, such as aflatoxins, rye ergot, castor-oil plant and crotalaria in feed materials
- 6.3. Preparation of aggregate samples
- 6.3.A. In relation to the control of substances or products distributed uniformly throughout the feed
- 6.3.B. In relation to the control of undesirable substances or products likely to be distributed non-uniformly throughout the feed, such as aflatoxins, rye ergot, castor-oil plant and crotalaria in feed materials
- 6.4. Preparation of final samples
- 6.5. Packaging of final samples
- 7. SAMPLING RECORD
- 8. DESTINATION OF SAMPLES
- ANNEX II
- GENERAL PROVISIONS ON METHODS OF ANALYSIS FOR FEED
- A. PREPARATION OF SAMPLES FOR ANALYSIS
- 1. Purpose
- 2. Precautions to be taken
- 3. Procedure
- 3.1. Feed which can be ground as such
- 3.2. Feed which can be ground after drying
- 3.3. Liquid or semi-liquid feed
- 3.4. Other feed
- 4. Storage of samples
- B. PROVISIONS RELATING TO REAGENTS AND APPARATUS USED IN METHODS OF ANALYSIS
- C. APPLICATION OF METHODS OF ANALYSIS AND EXPRESSION OF THE RESULTS
- 1. Extraction procedure
- 2. Clean-up procedure
- 3. Reporting of the method of analysis used
- 4. Number of determinations
- 5. Reporting of the analytical result
- 6. Measurement uncertainty and recovery rate in case of analysis of undesirable substances
- ANNEX III
- METHODS OF ANALYSIS TO CONTROL THE COMPOSITION OF FEED MATERIALS AND COMPOUND FEED
- A. DETERMINATION OF MOISTURE
- 1. Purpose and Scope
- 2. Principle
- 3. Apparatus
- 4. Procedure
- 4.1. Preparation
- 4.1.1.
- Feed other than those coming under 4.1.2 and 4.1.3
- 4.1.2.
- Cereals and groats
- 4.1.3.
- Feed in liquid or paste form, feed predominantly composed of oils and fats
- 4.2. Drying
- 4.2.1.
- Feed other than those coming under 4.2.2 and 4.2.3
- 4.2.2.
- Cereals, flour, groats and meal
- 4.3. Preliminary drying
- 4.3.1.
- Feed other than those coming under 4.3.2
- 4.3.2.
- Cereals
- 5. Calculation of results
- 5.1. Drying without preliminary drying
- 5.2. Drying with preliminary drying
- 5.3. Repeatability
- 6. Observation
- B. DETERMINATION OF MOISTURE IN ANIMAL AND VEGETABLE FATS AND OILS
- 1. Purpose and scope
- 2. Principle
- 3. Apparatus
- 4. Procedure
- 5. Calculation of results
- Repeatability
- C. DETERMINATION OF THE CONTENT OF CRUDE PROTEIN
- 1. Purpose and scope
- 2. Principle
- 3. Reagents
- 4. Apparatus
- 5. Procedure
- 5.1. Digestion
- 5.2. Distillation
- 5.2.1.
- Distillation into sulphuric acid
- 5.2.2.
- Distillation into boric acid
- 5.3. Titration
- 5.3.1.
- Sulphuric acid
- 5.3.2.
- Boric acid
- 5.4. Blank test
- 6. Calculation of results
- 6.1. Calculation for titration according to 5.3.1
- 6.2. Calculation for titration according to 5.3.2
- 6.2.1.
- Titration with hydrochloric acid
- 6.2.2.
- Titration with sulphuric acid
- 7. Verification of the method
- 7.1. Repeatability
- 7.2. Accuracy
- 8. Observations
- D. DETERMINATION OF UREA
- 1. Purpose and scope
- 2. Principle
- 3. Reagents
- 4. Apparatus
- 5. Procedure
- 5.1. Analysis of sample
- 5.2. Calibration curve
- 6. Calculation of results
- 7. Observations
- E. DETERMINATION OF VOLATILE NITROGENOUS BASES
- I. BY MICRODIFFUSION
- 1.
- Purpose and scope
- 2.
- Principle
- 3.
- Reagents
- 4.
- Apparatus
- 5.
- Procedure
- 6.
- Calculation of results
- Repeatability
- 7.
- Observation
- CONWAY CELL
- Scale 1/1
- II. BY DISTILLATION
- 1.
- Purpose and Scope
- 2.
- Principle
- 3.
- Reagents
- 4.
- Apparatus
- 5.
- Procedure
- 6.
- Calculation of results
- Repeatability
- F. DETERMINATION OF AMINO ACIDS (EXCEPT TRYPTOPHANE)
- 1. Purpose and scope
- 2. Principle
- 2.1. Free amino acids
- 2.2. Total amino acids
- 3. Reagents
- 4. Apparatus
- 5. Procedure
- 5.1. Preparation of the sample
- 5.2. Determination of free amino acids in feed and premixtures
- 5.3. Determination of total amino acids
- 5.3.1.
- Oxidation
- 5.3.2.
- Hydrolysis
- 5.3.2.1.
- Hydrolysis of oxidised samples
- 5.3.2.2.
- Hydrolysis of unoxidised samples
- 5.3.2.3.
- Open hydrolysis
- 5.3.2.4.
- Closed Hydrolysis
- 5.3.3.
- Adjustment of pH
- 5.3.3.1.
- For Chromatographic Systems (4.9) requiring a low sodium concentration
- 5.3.3.2.
- For all other Amino Acid Analysers (4.9)
- 5.3.4.
- Sample solution for chromatography
- 5.4. Chromatography
- 6. Calculation of results
- 7. Evaluation of the method
- 7.1. Repeatability
- 7.2 Reproducibility
- 8. Use of reference materials
- 9. Observations
- G. DETERMINATION OF TRYPTOPHAN
- 1. Purpose and scope
- 2. Principle
- 3. Reagents
- 4. Apparatus
- 5. Procedure
- 5.1. Preparation of samples
- 5.2. Determination of free tryptophan (extract)
- 5.3. Determination of total tryptophan (hydrolysate)
- 5.4. HPLC determination
- 6. Calculation of results
- 7. Repeatability
- 8. Results of a collaborative study
- 9. Observations
- H. DETERMINATION OF CRUDE OILS AND FATS
- 1. Purpose and scope
- 1.1. Procedure A — Directly extractable crude oils and fats
- 1.2. Procedure B — Total crude oils and fats
- 1.3. Interpretation of results
- 2. Principle
- 2.1. Procedure A
- 2.2. Procedure B
- 3. Reagents
- 4. Apparatus
- 5. Procedure
- 5.1. Procedure A (see point 8.1)
- 5.2. Procedure B
- 6. Expression of result
- 7. Repeatability
- 8. Observations
- I. DETERMINATION OF CRUDE FIBRE
- 1. Purpose and scope
- 2. Principle
- 3. Reagents
- 4. Apparatus
- 5. Procedure
- 6. Calculation of results
- 7. Repeatability
- 8. Observations
- J. DETERMINATION OF SUGAR
- 1. Purpose and scope
- 2. Principle
- 3. Reagents
- 4. Apparatus
- 5. Procedure
- 5.1. Extraction of sample
- 5.2. Determination of reducing sugars
- 5.3. Determination of total sugars after inversion
- 5.4. Titration by the Luff-Schoorl method
- 6. Calculation of results
- 7. Special procedures
- 8. Observations
- Example:
- K. DETERMINATION OF LACTOSE
- 1. Purpose and scope
- 2. Principle
- 3. Reagents
- 4. Apparatus
- 5. Procedure
- 6. Calculation of results
- 7. Observation
- L. DETERMINATION OF STARCH
- POLARIMETRIC METHOD
- 1.
- Purpose and scope
- 2.
- Principle
- 3.
- Reagents
- 4.
- Apparatus
- 5.
- Procedure
- 5.1. Preparation of the sample
- 5.2. Determination of the total optical rotation (P or S) (see observation 7.1)
- 5.3. Determination of the optical rotation (P' or S') of substances soluble in 40 % ethanol
- 6.
- Calculation of results
- 6.1. Measurement by polarimeter
- 6.2.
- Measurement by saccharimeter
- 6.3. Repeatability
- 7.
- Observations
- M. DETERMINATION OF CRUDE ASH
- 1. Purpose and Scope
- 2. Principle
- 3. Reagents
- 4. Apparatus
- 5. Procedure
- 6. Calculation of results
- 7. Observations
- N. DETERMINATION OF ASH WHICH IS INSOLUBLE IN HYDROCHLORIC ACID
- 1. Purpose and Scope
- 2. Principle
- 3. Reagents
- 4. Apparatus
- 5. Procedure
- 5.1. Method A
- 5.2. Method B
- 6. Calculation of results
- 7. Observation
- O. DETERMINATION OF CARBONATES
- 1. Purpose and Scope
- 2. Principle
- 3. Reagents
- 4. Apparatus
- 5. Procedure
- 6. Calculation of results
- 7. Observations
- P. DETERMINATION OF TOTAL PHOSPHORUS
- PHOTOMETRIC METHOD
- 1.
- Purpose and Scope
- 2.
- Principle
- 3.
- Reagents
- 4.
- Apparatus
- 5.
- Procedure
- 5.1. Preparation of the solution
- 5.1.1.
- Usual procedure
- 5.1.2.
- Samples containing organic substances and free from calcium and magnesium dihydrogen phosphates
- 5.2. Development of coloration and measurement of optical density
- 5.3. Calibration curve
- 6.
- Calculation of results
- Repeatability
- Q. DETERMINATION OF CHLORINE FROM CHLORIDES
- 1. Purpose and Scope
- 2. Principle
- 3. Reagents
- 4. Apparatus
- 5. Procedure
- 5.1. Preparation of the solution
- 5.1.1.
- Samples free from organic matter
- 5.1.2.
- Samples containing organic matter, excluding the products listed under 5.1.3.
- 5.1.3.
- Cooked feed, flax cakes and flour, products rich in flax flour and other products rich in mucilage or in colloidal substances (for example, dextrinated starch)
- 5.2. Titration
- 6. Calculation of results
- 7. Observations
- ANNEX IV
- METHODS OF ANALYSIS TO CONTROL THE LEVEL OF AUTHORISED ADDITIVES IN FEED
- A. DETERMINATION OF VITAMIN A
- 1. Purpose and Scope
- 2. Principle
- 3. Reagents
- 4. Apparatus
- 5. Procedure
- 5.1. Preparation of the sample
- 5.2. Saponification
- 5.3. Extraction
- 5.3.1.
- Extraction using a separating funnel (4.2.3)
- 5.3.2.
- Extraction using an extraction apparatus (4.8)
- 5.4. Preparation of the sample solution for HPLC
- 5.5. Determination by HPLC
- HPLC conditions
- 5.6. Calibration
- 5.6.1.
- Preparation of the working standard solutions
- 5.6.2.
- Preparation of the calibration solutions and calibration graph
- 5.6.3.
- UV standardisation of the standard solutions
- 5.6.3.1.
- Vitamin A acetate stock solution
- 5.6.3.2.
- Vitamin A palmitate stock solution
- 5.6.3.3.
- Vitamin A working standard solution
- 6. Calculation of the results
- 7. Observations
- 8. Repeatability
- 9. Results of a collaborative study
- (1)
- B. DETERMINATION OF VITAMIN E
- 1. Purpose and Scope
- 2. Principle
- 3. Reagents
- 4. Apparatus
- 5. Procedure
- 5.1. Preparation of the sample
- 5.2. Saponification
- 5.3. Extraction
- 5.3.1.
- Extraction using a separating funnel (4.2.3)
- 5.3.2.
- Extraction using an extraction apparatus (4.8)
- 5.4. Preparation of the sample solution for HPLC
- 5.5. Determination by HPLC
- HPLC conditions
- 5.6. Calibration (DL-α-tocopherol acetate or DL-α-tocopherol)
- 5.6.1.
- DL-α-tocopherol acetate standard
- 5.6.1.1.
- Preparation of the working standard solution
- 5.6.1.2.
- Preparation of the calibration solutions and calibration graph
- 5.6.1.3.
- UV standardisation of the DL-α-tocopherol acetate stock solution (3.10.1)
- 5.6.2.
- DL-α-tocopherol standard
- 5.6.2.1.
- Preparation of the working standard solution
- 5.6.2.2.
- Preparation of the calibration solutions and calibration graph
- 5.6.2.3.
- UV standardisation of the DL-α-tocopherol stock solution (3.11.1)
- 6. Calculation of the results
- 7. Observations
- 8. Repeatability·
- 9. Results of a collaborative study
- (2)
- C. DETERMINATION OF THE TRACE ELEMENTS IRON, COPPER, MANGANESE AND ZINC
- 1. Purpose and scope
- 2. Principle
- 3. Reagents
- Introductory comments
- 4. Apparatus
- 5. Procedure
- (3)
- 5.1. Samples containing organic matter
- 5.1.1.
- Ashing and preparation of the solution for analysis
- (4)
- 5.1.2.
- Spectrophotometric determination
- 5.1.2.1.
- Preparation of calibration solutions
- Iron
- Copper
- Manganese
- Zinc
- 5.1.2.2.
- Preparation of solution for analysis
- 5.1.2.3.
- Blank experiment
- 5.1.2.4.
- Measurement of the atomic absorption
- 5.2. Mineral feed
- 6. Calculation of results
- 7. Repeatability
- 8. Observation
- D. DETERMINATION OF HALOFUGINONE
- 1. Purpose and scope
- 2. Principle
- 3. Reagents
- 4. Apparatus
- 5. Procedure
- 5.1. General
- 5.2. Extraction
- 5.3. Clean up
- 5.3.1.
- Preparation of the Amberlite column
- 5.3.2.
- Sample clean up
- 5.4. HPLC determination
- 5.4.1.
- Parameters
- 5.4.2.
- Calibration graph
- 5.4.3.
- Sample solution
- 6. Calculation of results
- 7. Validation of the results
- 7.1. Identity
- 7.1.1.
- Co-chromatography
- 7.1.2.
- Diode-array detection
- 7.2. Repeatability
- 7.3. Recovery
- 8. Results of a collaborative study
- E. DETERMINATION OF ROBENIDINE
- 1. Purpose and scope
- 2. Principle
- 3. Reagents
- 4. Apparatus
- 5. Procedure
- 5.1. General
- 5.2. Extraction
- 5.3. Purification
- 5.3.1.
- Preparation of the aluminium-oxide column
- 5.3.2.
- Sample purification
- 5.4. HPLC determination
- 5.4.1.
- Parameters
- 5.4.2.
- Calibration graph
- 5.4.3.
- Sample solution
- 6. Calculation of results
- 7. Validation of the results
- 7.1. Identity
- 7.1.1.
- Co-chromatography
- 7.1.2.
- Diode-array detection
- 7.2. Repeatability
- 7.3. Recovery
- 8. Results of a collaborative study
- F. DETERMINATION OF DICLAZURIL
- 1. Purpose and scope
- 2. Principle
- 3. Reagents
- 4. Apparatus
- 5. Procedure
- 5.1. General
- 5.1.1.
- Blank feed
- 5.1.2.
- Recovery test
- 5.2. Extraction
- 5.2.1.
- Feed
- 5.2.2.
- Premixtures
- 5.3. HPLC determination
- 5.3.1.
- Parameters
- 5.3.2.
- Calibration solution
- 5.3.3.
- Sample solution
- 6. Calculation of the results
- 6.1. Feeds
- 6.2. Premixtures
- 7. Validation of the results
- 7.1. Identity
- 7.1.1.
- Co-chromatography
- 7.1.2.
- Diode-array detection
- 7.2. Repeatability
- 7.3. Recovery
- 8. Results of a collaborative study
- 9. Observations
- G. DETERMINATION OF LASALOCID SODIUM
- 1. Purpose and scope
- 2. Principle
- 3. Reagents
- 4. Apparatus
- 5. Procedure
- 5.1. General
- 5.1.1.
- Blank feed
- 5.1.2.
- Recovery test
- 5.2. Extraction
- 5.2.1.
- Feed
- 5.2.2.
- Premixtures
- 5.3. HPLC determination
- 5.3.1.
- Parameters
- 5.3.2.
- Calibration graph
- 5.3.3.
- Sample solution
- 6. Calculation of results
- 6.1. Feed
- 6.2. Premixtures
- 7. Validation of the results
- 7.1. Identity
- 7.1.1.
- Co-chromatography
- 7.2. Repeatability
- 7.3. Recovery
- 8. Results of a collaborative study
- ANNEX V
- METHODS OF ANALYSIS TO CONTROL UNDESIRABLE SUBSTANCES IN FEED
- A. DETERMINATION OF FREE AND TOTAL GOSSYPOL
- 1. Purpose and scope
- 2. Principle
- 3. Reagents
- 4. Apparatus
- 5. Procedure
- 5.1.
- Test sample
- 5.2.
- Determination of free gossypol
- 5.3.
- Determination of total gossypol
- 6. Calculation of results
- 6.1.
- From the specific optical density
- 6.2.
- From a calibration curve
- 6.2.1.
- Free gossypol
- 6.2.2.
- Total gossypol
- 6.3.
- Repeatability
- (B) DETERMINATION OF THE LEVELS OF DIOXINS (PCDD/PCDF) AND DIOXIN-LIKE PCBs
- I. METHODS OF SAMPLING AND INTERPRETATION OF ANALYTICAL RESULTS
- 1. Purpose and scope
- 2. Compliance of the lot or sublot with the specification
- II. SAMPLE PREPARATION AND REQUIREMENTS FOR METHODS OF ANALYSIS USED IN OFFICAL CONTROL OF THE LEVELS OF DIOXINS (PCDD/PCDF) AND DIOXIN-LIKE PCBs
- 1. Objective and field of application
- 2. Background
- 3. Quality assurance requirements to be complied with for sample preparation
- 4. Requirements for laboratories
- 5. Requirements for the analytical procedures for dioxins and dioxin-like PCBS
- Basic requirements for acceptance of analytical procedures:
- 6. Specific requirements for gc/ms methods to be complied with for screening or confirmatory purposes.
- 7. Screening methods of analysis
- 7.1. Introduction
- Screening approach
- Quantitative approach
- 7.2. Requirements for methods of analysis used for screening
- 7.3. Specific requirements for cell based bioassays
- 7.4. Specific requirements for kit based bioassays
- 8. Reporting of results
- ANNEX VI
- METHODS OF ANALYSIS FOR THE DETERMINATION OF CONSTITUENTS OF ANIMAL ORIGIN FOR THE OFFICIAL CONTROL OF FEED
- Conditions for the microscopic detection, identification or estimation of constituents of animal origin in feed
- 1. Objective and field of application
- 2. Sensitivity
- 3. Principle
- 4. Reagents
- 4.1. Embedding agent
- 4.2. Rinsing agents
- 4.3. Concentrating agent
- 4.4. Staining reagents
- 4.5. Bleaching reagent
- 5. Equipment and accessories
- 6. Procedure
- 6.1. Identification of constituents of animal origin in the sieve fractions
- 6.2. Identification of constituents of animal origin from the concentrated sediment
- 6.3. Use of embedding agents and staining reagents.
- 6.4. Examination in feed possibly containing fishmeal
- 7. Calculation and evaluation
- 7.1. Estimated value of the percentage of bone fragments
- 7.2. Estimated value of constituents of animal origin
- 8. Expression of the result of the examination
- 9. Optional protocol for analysing fat or oil
- ANNEX VII
- METHOD OF CALCULATING THE ENERGY VALUE OF POULTRYFEED
- 1. Method of calculation and expression of energy value
- 2. Tolerances applicable to declared values
- 3. Expression of result
- 4. Sampling and analysis methods
- ANNEX VIII
- METHODS OF ANALYSIS TO CONTROL ILLEGAL PRESENCE OF NO LONGER AUTHORISED ADDITIVES IN FEED
- A. DETERMINATION OF METHYL BENZOQUATE
- 1. Purpose and scope
- 2. Principle
- 3. Reagents
- 4. Apparatus
- 5. Procedure
- 5.1. General
- 5.2. Extraction
- 5.3. Liquid-liquid partition
- 5.4. Ion-exchange chromatography
- 5.4.1.
- Preparation of the cation-exchange column
- 5.4.2.
- Column chromatography
- 5.5. Liquid-liquid partition
- 5.6. HPLC determination
- 5.6.1.
- Parameters
- 5.6.2.
- Calibration graph
- 5.6.3.
- Sample solution
- 6. Calculation of results
- 7. Validation of the results
- 7.1. Identity
- 7.1.1.
- Co-chromatography
- 7.1.2.
- Diode-array detection
- 7.2. Repeatability
- 7.3. Recovery
- 8. Results of a collaborative study
- B. DETERMINATION OF OLAQUINDOX
- 1. Purpose and scope
- 2. Principle
- 3. Reagents
- 4. Apparatus
- 5. Procedure
- 5.1. General
- 5.2. Extraction
- 5.3. HPLC determination
- 5.3.1.
- Parameters:
- 5.3.2.
- Calibration graph
- 5.3.3.
- Sample solution
- 6. Calculation of the results
- 7. Validation of the results
- 7.1. Identity
- 7.1.1.
- Co-chromatography
- 7.1.2.
- Diode array detection
- 7.2. Repeatability
- 7.3. Recovery
- 8. Results of a collaborative study
- 9. Observation
- C. DETERMINATION OF AMPROLIUM
- 1. Purpose and Scope
- 2. Principle
- 3. Reagents
- 4. Apparatus
- 5. Procedure
- 5.1. General
- 5.1.1.
- Blank feed
- 5.1.2.
- Recovery test
- 5.2. Extraction
- 5.2.1.
- Premixtures (content < 1 % amprolium) and feed
- 5.2.2.
- Premixtures (content ≥ 1 % amprolium)
- 5.3. HPLC determination
- 5.3.1.
- Parameters:
- 5.3.2.
- Calibration graph
- 5.3.3.
- Sample solution
- 6. Calculation of the results
- 7. Validation of the results
- 7.1. Identity
- 7.1.1.
- Co-chromatography
- 7.1.2.
- Diode array detection
- 7.2. Repeatability
- 7.3. Recovery
- 8. Results of a collaborative study
- 9. Observations
- D. DETERMINATION OF CARBADOX
- 1. Purpose and scope
- 2. Principle
- 3. Reagents
- 4. Apparatus
- 5. Procedure
- 5.1. General
- 5.1.1.
- Blank feed
- 5.1.2.
- Recovery test
- 5.2. Extraction
- 5.2.1.
- Feed
- 5.2.2.
- Premixtures (0,1 %-2,0 %)
- 5.2.3.
- Preparations (> 2 %)
- 5.3. Purification
- 5.3.1.
- Preparation of the aluminium oxide column
- 5.3.2.
- Sample purification
- 5.4. HPLC determination
- 5.4.1.
- Parameters
- 5.4.2.
- Calibration graph
- 5.4.3.
- Sample solution
- 6. Calculation of the results
- 6.1. Feed
- 6.2. Premixtures and preparations
- 7. Validation of the results
- 7.1. Identity
- 7.1.1.
- Co-chromatography
- 7.1.2.
- Diode-array detection
- 7.2. Repeatability
- 7.3. Recovery
- 8. Results of a collaborative study
- ANNEX IX
- CORRELATION TABLES REFERRED TO IN ARTICLE 6
- 1. Directive 71/250/EEC
- 2. Directive 71/393/EEC
- 3. Directive 72/199/EEC
- 4. Directive 73/46/EEC
- 5. Directive 76/371/EEC
- 6. Directive 76/372/EEC
- 7. Directive 78/633/EEC
- 8. Directive 81/715/EEC
- 9. Directive 84/425/EEC
- 10. Directive 86/174/EEC
- 11. Directive 93/70/EEC
- 12. Directive 93/117/EC
- 13. Directive 98/64/EC
- 14. Directive 1999/27/EC
- 15. Directive 1999/76/EC
- 16. Directive 2000/45/EC
- 17. Directive 2002/70/EC
- 18. Directive 2003/126/EC
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